| 학회 |
한국공업화학회 |
| 학술대회 |
2012년 가을 (10/31 ~ 11/02, 대전컨벤션센터) |
| 권호 |
16권 2호 |
| 발표분야 |
포스터-나노 |
| 제목 |
Synthesis and characterization of double walled hollow nanoparticles using surface layer-by-layer assembly |
| 초록 |
In this paper, we introduce a three step; miniemulsion polymerization, condensation sol – gel method and thermal treatment synthesis of double walled hollow silica titania nanoparticles. The hollow silica nanoparticles were formed by sol-gel polymerization of TEOS precursor and calcination at 700℃ using styrene as template. Then another styrene layer was formed on the pre-synthesized hollow silica by miniemulsion polymerization. Subsequently, titania layer was formed on the hollow silica-styrene layer by polymerization of TBT precursor. Finally, the existing styrene layer was eliminated by calcination at 700℃ to obtain double walled hollow silica titania nanoparticles. The morphology and properties of the hollow nanoparticles were examined by TGA, FE-SEM, TEM and XRD. |
| 저자 |
김재균, 전순정, 김유나, SHAO GODLISTEN NAMWEL, 김희택
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| 소속 |
한양대 |
| 키워드 |
Hollow nanoparticles; Layer-by-layer assembly; miniemulsion polymerization; Sol-gel method
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| E-Mail |
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