화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2009년 봄 (04/23 ~ 04/24, 광주 김대중컨벤션센터)
권호 15권 1호, p.912
발표분야 재료
제목 Synthesis of Copper-doped Zinc Oxide Nanoparticles by Simple Solution Process
초록 Recently, doped ZnO nanoparticles have been extensively studied due to its wide applications in optical, electrical, and sensing devices. In this regard, first we synthesized ZnO nanoparticles with diameter ranges from 30-40 nm by using zinc acetate, NaOH, and hexamethylenetetramine (HMTA) at 90 0C for 3 h by simple solution process. Copper-doping in ZnO nanoparticles were performed through impregnation method using various weight percentage of copper, i.e. Zn1-xCuxO where X=0.01 (sample a), 0.02 (sample b), 0.03 (sample c), and 0.06 (sample d) at 600 0C. Copper-doped ZnO nanoparticles prepared with this techniques were characterized by FESEM, TEM, and EDS spectra. X-ray diffraction (XRD) results indicated that introduction of copper with atomic ration of x= 0.02 (samples a and b) showed no influence on the crystal structure of ZnO, but substantial effect with x=0.03 (samples c and d) was observed. Moreover, UV-Vis spectroscopy showed significant enhancement in the optical absorption compared with the un-doped ZnO nanoparticles.
저자 홍동민1, Mohammad Vaseem2, 한윤봉3
소속 1School of Semiconductor and Chemical Engineering, 2and BK 21 Centre for Future Energy Materials and Devices, 3Nanomaterials Processing Research Centre
키워드 Nanoparticles; Solution Process
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