화학공학소재연구정보센터
학회 한국고분자학회
학술대회 2005년 봄 (04/14 ~ 04/15, 전경련회관)
권호 30권 1호, p.494
발표분야 유ㆍ무기 나노섬유 소재
제목 Electrospinning of cellulose/NMMO monohydrate sloutions
초록 Research on spinning of cellulose made a significant progress in recent years. Electrospinning of cellulose in the NMMO monohydrate solvent was tried to achieve a new processing method for the cellulose nanofibers. The NMMO monohydrate is a good solvent for the cellulose.
Cellulose/NMMO monohydrate solution forms a solution at 80℃ and freezes again at room temperature. The injection tube was heated to 100℃ to maintain the solution state.
The process for preparing a cellulose solution by liquid N-methylmorpholine N-oxide monohydrate (NMMO monohydrate) solvent. Celulose powder( DP=850)and NMMO solvent were mixed and dissolved at 80 ℃. The cellulose/NMMO monohydrate solution was electrospun at 100℃. The cellulose concentrations were 0.5, 1, 2, 3, 4, 5 wt%. The distance between the needle tip to ground was 15 cm and the 15KV was applied for the electrospinning.



Fig. 1. Schematic diagram of electrospinning of
cellulose/NMMO monohydrate solution setup

References
1. D.B.Kim;S.M.Jo;W.S.Lee;J.J.Pak.Wiley Interscience DOI 10.1002/app.20607 (2004)
저자 권세력, 설창, 김태헌, 김진헌, 이준호
소속 인하대
키워드 Electrospinning ; cellulose; NMMO monohydrate
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