화학공학소재연구정보센터
학회 한국재료학회
학술대회 2020년 가을 (11/18 ~ 11/20, 휘닉스 제주 섭지코지)
권호 26권 1호
발표분야 A. 전자/반도체 재료 분과
제목 Fabrication of microcapsule latent curing agent via co-axial electrospray(CES) method
초록 The epoxy–imidazole resin system is used to form the flexible printed circuit board (FPCB) joining. The pot-life of the system is very significant to FPCB production. 2-phenylimidazole (2Pz) encapsulated particles were produced for the latent curing agent system to use in the reaction of epoxy resin. Polycaprolactone (PCL) was used as a wall material, and the electrospray method was used to fabricate the microcapsule. Stable process with spherical morphology of microcapsule was found with 3% of PCL polymer, voltage of 10kV, polymer federate of 0.5 mL/h, needle size of 0.26 cm, tip-to-collection (TTC) distance of 25 cm, and 2Pz concentration of 0.25 and 0.5%. The encapsulation rate was approximately 7.5%. The permeability test showed microcapsule released almost all of 2Pz content after 150 minutes.
저자 신인섭, 박준서
소속 한경대
키워드 Co-axial electrospray; epoxy resins; curing agent; polymer curing.
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