화학공학소재연구정보센터
학회 한국고분자학회
학술대회 2006년 봄 (04/06 ~ 04/07, 일산킨텍스)
권호 31권 1호
발표분야 복합재료
제목 Multiwall carbon nanotube with anchored phenol structures: Preparation, Characterization and its influence on the properties of phenolic resin composites
초록 Surface functionalization of multiwall carbon nanotube was carried out by introducing ylides groups containing anchored phenol structures on the surface. The functionalized nanotube is characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, thermogravimetric analysis and Raman spectroscopy. The formation of azomethine ylides is further confirmed from the peak at 1376 cm-1 and a small hump at 1279 cm-1 that’s are due to –CNC stretching and –CN stretching of tertiary amine group. Raman spectroscopic studies further corroborates that the surface functionalization does not affect the basic crystal domain size of the nanotubes. Thermogravimetric analysis exhibits higher weight loss supporting the chemical functionalization. The functionalized carbon nanotubes were then incorporated in phenolic resin (Novalac resin) and its influence on the curing kinetics, flexural strength and electrical conductivity were determined.
저자 노우현, 샨묵하라즈, 신동준, 이광용, 이세형, 류승훈
소속 경희대
키워드 Multiwall carbon nanotube; phenolic resin; Raman spectroscopy; curing kinetics
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