| 학회 |
한국화학공학회 |
| 학술대회 |
2008년 가을 (10/23 ~ 10/24, 부산 BEXCO) |
| 권호 |
14권 2호, p.3316 |
| 발표분야 |
재료 |
| 제목 |
Continuous synthesis of surface-modified zinc oxide nanoparticles using supercritical methanol |
| 초록 |
Surface-modified zinc oxide (ZnO) with diameters less than 400 nm were synthesized rapidly and continuously in supercritical methanol at temperature 400oC and at pressure 30 MPa by using a flow type reactor system. Wide angle X-ray diffraction (WAXD) analysis revealed that the surface-modified nanoparticles had ZnO crystalline structure. Dispersion test in solvents and transmission electron microscopy (TEM) analyses showed that the addition of organic modifier into the reaction system significantly affected the morphology and dispersion stability of nanocrystals. The results of fourier transform infrared (FTIR) demonstrated that reagents chemically bounded onto the surface of ZnO nanoparticles. |
| 저자 |
밤방, 박현채, 김재훈, 김재덕
|
| 소속 |
KIST |
| 키워드 |
zinc oxide; nanoparticles; surface modification
|
| E-Mail |
|
| 원문파일 |
초록 보기 |
