| 초록 |
We have synthesized nanostructured, organic-inorganic hybrid mesoporous materials using sol-gel procedure by co-condensation of 1,2-(triethoxysilyl)ethane (BTESE) and (3-cyanopropyl)triethoxysialne (3-CPS) under basic conditions, using cetyltrimethylammonium bromide (CTAB) as a structure directing agent. The solvent extracted resulting materials were characterized by X-ray diffraction (XRD), Nitriogen gas sorption, Fourier transform infrared spectroscopy (FT-IR), Thermogravimteric analysis (TGA) and Scanning electron microscope (SEM). The choice of reaction variable and loading effect of 3-CPS will be discussed in this paper. |
