학회 | 한국공업화학회 |
학술대회 | 2016년 봄 (05/02 ~ 05/04, 여수 엑스포 컨벤션) |
권호 | 20권 1호 |
발표분야 | 정밀화학_포스터 |
제목 | Synthesis and Single-crystal X-ray Characterization of Tetrakis(5,5-dimethyl-2,2-diphenyl-1,3-dioxane)germanium |
초록 | We reacted germanium tetrachloride with 2-(4-bromophenyl)-5,5-dimethyl-2-phenyl-1,3-dioxane organolithium to obtain tetrakis(5,5-dimethyl-2,2-diphenyl-1,3-dioxane)germanium. Recrystallization of the germanium compound from toluene gave a clear needle-shaped crystal. Molecular structure of this compound was analyzed by nuclear magnetic resonance spectrometer and single crystal X-ray diffractometer. |
저자 | 이태원, 신주석, 이지영, 이하나, 박광용 |
소속 | 중앙대 |
키워드 | tetrakis(5; 5-dimethyl-2; 2-diphenyl-1; 3-dioxane)germanium; structure analysis; single crystal structure; tetragonal |