| 학회 |
한국고분자학회 |
| 학술대회 |
2014년 가을 (10/06 ~ 10/08, 제주 ICC) |
| 권호 |
39권 2호 |
| 발표분야 |
고분자가공/복합재료-자가치유 고분자와 복합소재 |
| 제목 |
Preparationand Characterization of Polyacrylonitrile-based Carbon Fibers Produced byElectron Beam Irradiation Pretreatment |
| 초록 |
This study evaluated the feasibility of polyacrylonitrile (PAN) fibers stabilized by thermal treatment after electron beam irradiation(EBI) in the production of carbon fibers. The effects of EBI and thermal treatments on the PAN precursor were verified by FT-IR, differential scanning calorimetry (DSC), X-ray diffraction (XRD), and scanning electron microscopy (SEM). FT-IR spectra confirmed that the intensities of the C≡N stretching vibration at 2244 cm-1 significantly decreased as the thermal treatment temperature increase from 200°C to 250°C and the holding time from 20 min to 40 min after EBI process. The stabilization index (SI) values for the PAN fibers that were exposed to EBI and thermal treatment after EBI were evaluated by XRD. The SI value of the PAN fibers that were treated at 250 °C for 40 min after EBI was 99.21%. |
| 저자 |
신혜경1, 박미라2, 김학용2, 박수진1
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| 소속 |
1인하대, 2전북대 |
| 키워드 |
electron beam irradiation; polyacrylonitrile; stabilization; pretreatment
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| E-Mail |
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