In the present work, the plasma nitriding behavior of a nickel based dental alloy was investigated. Plasma nitriding experiments carried out under constant gas mixture (15% H(2)-85% N(2)) for different process parameters including time (4, 6, 10, and 20 h) and temperature (400, 450, 500, and 550 A degrees C). Depending on nitriding parameters, it was found that triple or double layers formed on the surface of the samples. Increasing of treatment time and temperature has resulted in a double layer. gamma(N1) layer was in formed all nitrided samples. However, gamma(N2) layer is formed only at low temperatures and in short times. Layer growth of nickel based alloys increases until a critical time or a critical temperature reached. Above these critical values, it is observed that the layer thickness decreases. It was also found that plasma nitriding not only increases the surface hardness but also improves the wear resistance of nickel based dental alloy. The maximum wear resistance was observed at 400 A degrees C for 10 h due to the high hardness and thickness of the nitride layers.