화학공학소재연구정보센터
Materials Science Forum, Vol.495-497, 761-766, 2005
A study of the early stages of recovery in cold rolled {110}< 001 > oriented copper single crystals
Copper single crystals of {110}(001) crystallographic orientation were cold rolled to a true strain of 1.4. Specimens were cut from the as-deformed crystals with all surfaces mechanically ground and deep-etched in concentrated nitric acid to minimise the likelihood of surface nucleation of recrystallized grains during subsequent annealing. The early stages of static recovery were studied by annealing specimens at 300 degrees C. The crystallographic features of the deformed and annealed microstructures were determined by high resolution electron backscatter diffraction. It was observed that deformation was homogeneous with the microstructure in ND-RD plane exhibiting two complementary sets of intersecting bands at similar to +/- 35 degrees to ND. Along these bands and in the microstructure, in general, there was an overall spread in orientation about ND towards {110}(112). However, the orientation spread along these bands was cyclic, that is, sinusoidal orientation gradients were generated about ND with amplitude of up to 20 degrees and wavelength 5-10 mum. Annealing resulted in, the preferred growth of cells that have orientations at the edge of the orientation spread of the deformation substructure. This localized coarsening of the microstructure is similar to the discontinuous subgrain growth observed in {110}(001) oriented Al single crystals and indicates that discontinuous subgrain (cellular) growth can also occur in metals of lower stacking fault energy.