화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Korean Journal of Chemical Engineering, Vol.34, No.3, 723-733, March, 2017
DOI10.1007/s11814-016-0311-3  Export Citation
A novel hydrothermal releasing synthesis of modified SiO2 material and its application in phenol removal process
Xinyu Yang, Xiaoyao Liu, Wenjing Tang, Yajun Gao, Huijuan Ni, and Jianbin Zhang†
  • College of Chemical Engineering, Inner Mongolia University of Technology, Hohhot 010051, China
E-mail:
A modified SiO2 material (MSM) was successfully synthesized by using Na2SiO3 and a novel CO2SM in the presence of CTAB through an innovative hydrothermal releasing treatment protocol. The MSM was systemically characterized using several techniques, including N2 adsorption-desorption isotherm, thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The CO2SM as a platform for CO2 capturing and releasing can be reversibly used for multiple cycles without significant loss of capabilities. The optimum conditions for the preparation of MSM were identified as follows: Na2SiO3 concentration, 0.2mol/L; hydrothermal temperature, 120 °C; CO2SM dosage, 6 g; CTAB concentration, 24 g/L, reaction time, 12 h. Additionally, the MSM exhibited high efficiency for the removal of phenol from aqueous solution: it showed a phenol adsorption capacity of 91.29mg/g when shaken with the aqueous phenol solution at 180 rpm for 1 h at 25 °C.
Keywords:MSM;CO2SM;Hydrothermal Releasing Method;Adsorption;Phenol
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