화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Journal of Industrial and Engineering Chemistry, Vol.107, 145-154, March, 2022
DOI10.1016/j.jiec.2021.11.041  Export Citation
Microwave-assisted polycrystalline Ag/AgO/AgCl nanocomposites synthesis using banana corm (rhizome of Musa sp.) extract: Characterization and antimicrobial studies
Krishna Kumar Jaiswal1, †, Ishita Banerjee2, Swapnamoy Dutta3, Ravikant Verma4, Lokanadhan Gunti5, Sharad Awasthi6, Mayank Bhushan7, †, Vinod Kumar8, 9, †, Mohamed Fahad Alajmi10, and Afzal Hussain10
  • 1Institute for Water and Wastewater Technology, Durban University of Technology, Durban 4000, South Africa
  • 2Department of Biochemistry & Cellular and Molecular Biology, The University of Tennessee, Knoxville, TN 37996, USA
  • 3Department of Green Energy Technology, Pondicherry University, Puducherry 605014, India
  • 4Department of Ecology and Environmental Sciences, Pondicherry University, Puducherry 605014, India
  • 5Department of Microbiology, Pondicherry University, Puducherry 605014, India
  • 6Department of Biotechnology, Pondicherry University, Puducherry 605014, India
  • 7Department of Nanotechnology, North-Eastern Hill University, Shillong, Meghalaya 793022, India
  • 8Department of Life Sciences, Graphic Era (Deemed to Be University), Dehradun, Uttarakhand 248002, India
  • 9Peoples’ Friendship University of Russia (RUDN University), Moscow 117198, Russian Federation
  • 10Department of Pharmacognosy, College of Pharmacy, King Saud University, PO Box 2457, Riyadh 11451, Saudi Arabia
E-mail:, ,
The rapid emergence of multidrug-resistant microbes has turned into the main threat to public health worldwide. The preparation and application of nanomaterial-based antimicrobials have increased to address this problem with great significance. This study has investigated the bio-fabrication of polycrystalline Ag-NCs using BCE as a reducer and stabilizer under microwave irradiation. Ag-NCs formations were optimized using varying concentrations of BCE and silver acetate. The XRD confirmed the incidence of phases of nanostructured crystals of Ag/AgO/AgCl. The average crystallite sizes were calculated to be 22.19, 36.65, and 36.65 nm for Ag, AgO, and AgCl, respectively. SERS spectra revealed the vibrational modes of the Ag and Ag-O stretch bands. FTIR spectra have indicated the incidence of chemical fingerprints for Ag-NCs and BCE biomolecules. SEM and HR-TEM micrographs exhibited the almost spherical to the oval shape of ∼50 nm. SAED pattern attested to silver crystallinity in agreement with XRD analysis. The MIC values of the Ag-NCs against Escherichia coli, Staphylococcus aureus, Aspergillus brasiliensis, and Rhizopus stolonifer were observed to be 120, 60, 200, and 100 µg/ml, respectively. This study has demonstrated the facile method to prepare polycrystalline Ag-NCs with appropriate structural and morphological characteristics for antimicrobial applications.
Keywords:Microwave irradiation;Bio-fabrication;Silver nanoparticles;Banana corm extract;Antimicrobial activities
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