화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Macromolecular Research, Vol.16, No.7, 575-585, October, 2008
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Small-Angle X-ray Scattering Station 4C2 BL of Pohang Accelerator Laboratory for Advance in Korean Polymer Science
Jinhwan Yoon, Kwang-Woo Kim†, Jehan Kim, Kyuyoung Heo, Kyeong Sik Jin, Sangwoo Jin, Tae Joo Shin, Byeongdu Lee, Yecheol Rho, Byungcheol Ahn, and Moonhor Ree†
  • Pohang Accelerator Laboratory, Dept. of Chemistry, National Lab for Polymer Synthesis & Physics, Center for IntegratedMolecular Systems, and Polymer Research Institute, Pohang University of Science and Technology, Pohang 790-784, Korea
E-mail:,
There are two beamlines (BLs), 4C1 and 4C2, at the Pohang Accelerator Laboratory that are dedicated to small angle X-ray scattering (SAXS). The 4C1 BL was constructed in early 2000 and is open to public users, including both domestic and foreign researchers. In 2003, construction of the second SAXS BL, 4C2, was complete and commissioning and user support were started. The 4C2 BL uses the same bending magnet as its light source as the 4C1 BL. The 4C1 BL uses a synthetic double multilayer monochromator, whereas the 4C2 BL uses a Si(111) double crystal monochromator for both small angle and wide angle X-ray scattering. In the 4C2 BL, the collimating mirror is positioned behind the monochromator in order to enhance the beam flux and energy resolution. A toroidal focusing mirror is positioned in front of the monochromator to increase the beam flux and eliminate higher harmonics. The 4C2 BL also contains a digital cooled charge coupled detector, which has a wide dynamic range and good sensitivity to weak scattering, thereby making it suitable for a range of SAXS and wide angle X-ray scattering experiments. The general performance of the 4C2 BL was initially tested using standard samples and further confirmed by the experience of users during three years of operation. In addition, several grazing incidence X-ray scattering measurements were carried out at the 4C2 BL.
Keywords:small-angle X-ray scattering;wide-angle X-ray scattering;in-situ X-ray scattering;transmission X-ray scattering;grazing-incidence X-ray scattering;synchrotron radiation sources;Pohang Accelerator Laboratory;beamline;detector;polymers
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