Journal of Industrial and Engineering Chemistry, Vol.36, 132-138, April, 2016
12HPW/meso-SiO2 nanocomposite CSPEEK membranes for proton exchange membrane fuel cells
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In this study, cross-linked sulfonated poly(ether ether ketone) (CSPEEK) membranes with 10 wt% HPW/meso-SiO2 nanoparticles were prepared using an electron beam irradiation method at a dose of 300 kGy. The prepared membranes were characterized using the gel fraction, TGA, and SAXS, water uptake, ion exchagne capacity, and proton conductivity. The proton conductivity of a nanocomposite SPEEK membrane with 20 wt% HPW/meso-SiO2 nanoparticle was 1.9 × 10-3 S/cm at 120 °C under 30% RH, and which is 10 times higher than the CSPEEK membrane without the nanoparticles.
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